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The reference phase is adjusted by the operator so that it is exactly in phase with the NMR signal when the condition of exact resonance is attained, that is, at the exact center of the NMR line. 15 (A) Block diagram of a simplified field-sweep system. 15 (B) Block diagram of a simplified frequency-sweep system. amplitude of the incoming NMR signal. Hence, at the center of the NMR peak, the pen reaches its highest position on the chart paper. If the reference input is adjusted so that its phase is 180° with respect to the signal, the spectrum appears inverted on the chart paper.

D. Department of Chemistry and Biochemistry, Montana State University, Bozeman, Montana Michael T. D. D. Department of Pharmacology, University of Texas Southwestern Medical Center at Dallas, Dallas, Texas Viswanathan Seshan, B. Tech. Graduate Program in Biomedical Engineering, University of Texas Southwestern Medical Center at Dallas, Dallas, Texas Daniel D. D. NMR Concepts and Department of Chemistry, University of Rhode Island, Kingston, Rhode Island Roderick E. D. Department of Chemistry, Dalhousie University, Halifax, Nova Scotia, Canada Page 1 1 NMR Concepts Daniel D.

MARTHA D. BRUCH Page v Contents Preface iii Contributors vii 1. NMR Concepts Daniel D. Traficante 1 2. Spectral Editing Methods for Structure Elucidation Martha D. Bruch and Cecil Dybowski 61 3. NMR Relaxation and Dynamics Roderick E. Wasylishen 105 4. Multidimensional NMR Spectroscopy of Liquids Martha D. Bruch 145 5. Small Organic Molecules: Practical Tips and Structure Elucidation Cynthia K. McClure 239 Page vi 6. Structure Determination of Biological Macromolecules Josep Rizo and Martha D. Bruch 285 7.

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